Benzyl Benzoate USP BP Ph Eur Suppliers & Exporters, CAS 120-51-4 |
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SDS MSDS of Benzyl Benzoate USP BP Ph Eur Manufacturers
Benzyl Benzoate
CAS Number 120-51-4, USP BP Ph Eur Commercial & Pure
Specifications of Benzyl Benzoate USP Grade
C14H12O2 -- 212.24 -- CAS 120-51-4.
Benzoic acid, phenylmethyl ester.
Benzyl Benzoate contains not less than 99.0 percent and not more than 100.5 percent of C14H12O2.
Identification: Infrared Absorption.
TESTS
Meets all the tests for Specifications of Benzyl Benzoate USP mongograph.
Specifications of Benzyl Benzoate BP Ph Eur Grade
C14H12O2 -- 212.2 -- CAS 120-51-4
DEFINITION
Phenylmethyl benzoate.
Content: 99.0 per cent to 100.5 per cent.
CHARACTERS
Appearance: Colourless or almost colourless crystals or colourless or almost colourless, oily liquid.
Solubility: Practically insoluble in water, miscible with ethanol (96 per cent), with methylene chloride and with fatty and essential oils.
IDENTIFICATION
First identification A.
Second identification B, C.
A. Infrared absorption spectrophotometry (2.2.24). Comparison Ph. Eur. reference spectrum of benzyl benzoate.
B. To 2 g add 25 ml of alcoholic potassium hydroxide solution and boil under a reflux condenser for 2 h. Remove the ethanol on a water-bath, add 50 ml of water and distill. Collect about 25 ml of distillate and use it for identification test C. Acidify the liquid remaining in the distillation flask with dilute hydrochloric acid. A white precipitate is formed that, when washed with water and dried in vacuum melts at 121C to 124C.
C. To the distillate obtained in identification test B add 2.5 g of potassium permanganate and 5 ml of dilute sodium hydroxide solution. Boil under a reflux condenser for 15 min, cool and filter. Acidify the filtrate with dilute hydrochloric acid. A white precipitate is formed that, when washed with water and dried in vacuum, melts at 121C to 124C.
TESTS
Meets all the tests for Specifications of Benzyl Benzoate BP Ph Eur mongograph.
Benzyl Benzoate USP BP Ph Eur Manufacturers:
Muby Group
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